A comparative study of lignocellulosic nanofibrils isolated from celery using oxalic acid hydrolysis followed by sonication and mechanical fibrillation

编号 020019305

推送时间 20190701

研究领域 林产化工 

年份 2019 

类型 期刊 

语种 英语

标题 A comparative study of lignocellulosic nanofibrils isolated from celery using oxalic acid hydrolysis followed by sonication and mechanical fibrillation

来源期刊 CELLULOSE

期 第193期

发表时间 20190426

关键词 Celery;  Lignocellulosic nanofibrils;  Oxalic acid hydrolysis;  Disk grinding; 

摘要 Two lignocellulosic nanofibrils (LCNF) were produced from celery using oxalic acid hydrolysis and sonication (OS) or refining by a SuperMassColloider grinder treatment (MT). Physicochemical properties, such as morphological properties, crystallinity, thermal stability, zeta potential and transmittance for the obtained nanofibrils were evaluated. Compared to refining in SuperMassColloider grinder, OS treatment contributed greater separation of nanofibril bundles by introducing negative carboxyl groups. In detail, mechanical fibrillation resulted in the LCNF with longer length and thicker diameter. OS treatment produced LCNF with smaller height of 5.5nm and higher aspect ratio than the one obtained by MT treatment, and endowed high crystallinity and thermal stability due to its preferential degradation of amorphous carbohydrates and lignin. Furthermore, OS-LCNF with carboxyl group contributed more stable aqueous suspension with surface charge of -32.9mV, better than MT-LCNF sample with entangled network structure. The comparative study can gain insight into the use of celery as a potential source for nanocellulose production.

服务人员 尚玮姣

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